MS Report from Instrument: LCMS-02 File ..621 2017-06-21 12-44-59\\CPK2017-621-13084.D Tgt Mass (CHM): Injection Date : 21 Jun 17 5:37 pm +0800 Seq. Line : 59 Sample Name : CPK2017-621-13084 Location : P2-D-02 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170621\\20170621 2017-06-21 12-44-59\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170621\\20170621 2017-06-21 12-44-59\\1-POS-3MIN.M Catalog No : HY-11000 Batch#13084 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off mAU80060040020001.6960.4411.2921.6540.5 DAD1 C, Sig=254,4 Ref=off mAU2000.445100011.51.69622.5min2.0780.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500001000005000001.51.72222.5min0.511.5 Ion 433.4, MSD1 433.4,Target Mass 432.4 +H Positive, EIC=433.1:434.1 10000075000500002500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.51.72122.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.44 0.02 1.60 1.42 0.13 ND 1.29 0.02 1.35 1.09 0.11 ND 1.65 0.02 7. 6.71 0.63 ND 1.70 0.02 1237.56 991.58 99.13 433 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.44 0.02 0.97 0.88 0.27 ND 1.70 0.03 357.31 288.41 99.43 433 2.08 0.02 1.07 0.82 0.30 233 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.72 0.03 3167.13 159095.78 100.00 433LCMS-02 6/21/2017 18:23:09 CLJ_701Page 1 of 2
MS Report from Instrument: LCMS-02Ret. Time: 1.72 <<<< POSITIVE SPECTRA >>>> ES-API Positive300002500020000 434.1150001000050000200300400500600700800900m/z 433.1 455.1 471.0LCMS-02 6/21/2017 18:23:09 CLJ_701 591.1Page 2 of 2
